20ml of catalyst will be loaded into the reactor.
The reactor will be purged with Nitrogen, at a rate of 2 scf/h and at 27 psig for 15 minutes
Adjust the reactor pressure to 430 psig with H2.
Establish a Hydrogen gas rate of 0,746 scf/h or 2965 scf/b.
Heat the reactor to 275oF at 45oF/h. (Max. allowable temperature 300oF)
Time to set point = 3h54 & check that H20 is negligible out of separator.
Спасибо